NMR Characterization of Flavanone Naringenin 7-O-Glycoside Diastereomer
To discriminate R and S Myrrh flavanone glycoside using NMR, the mixture of R and S naringenin 7-O-glycoside was first isolated from Gleditsia sinensis.1H and 13C NMR data of the mixture were recorded with 1H NMR, 13C NMR, 1H-1H COSY, 1H-13C HSQC and 1H-13C HMBC in DMSO-d6 solution.The two diastereomers were then separated with chiral chromatograph